| M0099027 | |
| Plastics / textiles | |
| 3 mm | |
| < 0,2 mm | |
| 50-100 g | |
| We recommend using a Variable Speed Rotor Mill PULVERISETTE 14 for a batch wise grinding of sample. |
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Variable Speed Rotor Mill PULVERISETTE 14 classic linerotor speed: 20.000 rpm impact rotor with 12 ribs made of stainless steel + sieve ring: 0.50 mm trapezoidal perforations made of stainless steel + accessories for grinding large quantities |
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pre grinding of sample | |
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100 g | |
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3 mm | |
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+ liquid nitrogen (N2) | |
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4 min | |
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< 0,5 mm | |
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For problematic thermoplastic samples, it might be beneficial to grind in steps. With our first trial, we used a 0,5 mm sieve ring for precutting. Afterwards, the sample can be ground with the desired 0,2 mm sieve ring.
We recommend using the accessories for grinding large quantities if samples amounts > 50 g should be ground. It is also possible to grind batch wise instead of using the accessories for grinding large quantities. Previously, sample has been placed into liquid nitrogen for embrittlement. After a minute of chilling, sample has been fed spoon by spoon to the feeding funnel.
This way, it took about 4 minutes to grind the entire sample amount. Only a bit of sample use to stick to the impact rotor or the sieve ring. Even higher amounts of sample can be ground this way.
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Variable Speed Rotor Mill PULVERISETTE 14 classic linerotor speed: 20.000 rpm impact rotor with 12 ribs made of stainless steel + sieve ring: 0.20 mm trapezoidal perforation stainless steel |
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50 g | |
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< 0.5 mm | |
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+ liquid nitrogen (N2) | |
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15 min | |
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< 0,2 mm | |
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The sample has been pre ground in result 1. Now, with a start size of < 0,5 mm, sample can be ground in a second grinding step to < 0,2 mm.
For this, sample has been placed back into liquid nitrogen for embrittlement. After ~ 1-2 minutes, we started feeding the pre ground sample to the feeding funnel.
It took about 15 minutes until 50 g of pre ground sample got ground with this kind of setting. Sieve ring and impact rotor are mainly free of residues. Therefore, even higher amounts of sample can be ground this way (use accessories for grinding large quantities when > 50 g of sample should be ground).
Because sample use to stay attached to pan and lid, we recommend vacuuming with a soft brush for rapid cleaning. |
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Universal Cutting Mill PULVERISETTE 19 Speed 300-3000 rpmstandard rotor with V-cutting edges and fixed knives made of tool steel + sieve cassette: 0.50 mm trapezoidal perforation made of stainless steel + sample exhauster system with cyclone separator |
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20 g | |
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3 mm | |
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5 min | |
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< 0,5 mm | |
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With the optional cyclone separator, air flow of ~ 2800 liters per minute will help to keep the sample chilled. With a sieve cassette of 0,5 mm trapezoidal perforation, we have been able to feed 20 g of sample within 5 minutes (low feed rate). After a total of 5 minutes, the sample started to melt inside the grinding chamber. An output of ~ 15 g of ground sample has been achieved.
An additional embrittlement with liquid nitrogen is not recommended with a cutting mill. The additional cooling effect will not last very long before the nitrogen use to be evaporated. We would recommend to grind the sample together with dry ice (CO2) which remains much longer in the grinding chamber. Unfortunately our application laboratory does not provide dry ice to testify the grindability of sample this way.
Melted pieces could be removed as a soft mass out of the grinding chamber. Rest of sample was attached by electrostatic charge and could be removed rapidly by using a vacuum cleaner and a soft brush.
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