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Sample which has been ground with Jaw Crusher PULVERISETTE 1 Model I in result 1 has been placed in liquid nitrogen again for embrittlement. After the sample has been chilled (~ 1 min), sample has been fed to the feeding funnel of Disk Mill PULVERISETTE 13 spoon wise.
After ~4-5 minutes, all sample has been ground. Majority of ground sample use to be < 1,5 mm. Because the grinding disks are barely free of residues, even higher amounts should be grindable.
Also smaller gap settings are plausible to achieve finer grinding results.
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