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After pre grinding the cake in result 1, we use the Disk Mill PULVERISETTE 13 for a grinding to the desired fineness.
For this, we set a gap of 150 µm and started grinding the complete pre ground sample from result 1.
After 5 minutes, the complete iron powder cake sample has been ground. There are no sticking residues between the grinding disks; for this, even higher amounts can be ground.
Because sample can pass the disks gap after 1 dimension of ground sample is < 150µm, we used our Vibratory Sieve Shaker ANALYSETTE 3 Pro and a test sieve with 200µm mesh (as desired) to determine the fineness by sieving of an aliquot.
With a gap setting of 150 µm, already 97,6 % of sample is passing a 200 µm mesh test sieve. It is possible to increase the amount of sample < 200 µm by setting a smaller gap (min. 100 µm should be set as gap).
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